Free Appendix - District Court of Delaware - Delaware

I Case1:05—cv-00443-GIVIS Document 3-7 Filed 06/28/2005 Page10f3
AppcndixM

Case A1 :05-cv-00443-G ix/iSAPl1¤eNDrI¤(@»i L Filed oe/as/zoos Page 2 er 3 P (
FPC DE FMAL EFFLUENT COIVIPOSITE SAMPLING AND -
FILE TESTING USED FOR WEEKLY NPDES SAMPLTNG Page 1 gf 2
` ` (Excerpted fiom FPC-DE Procedure OM269.010)
3.0 RESPONSIBILITY l ` _
l 3.1 alt is the responsibility of all Operators that are qualified and assigned to the W W IP to follow the procedure and to
cross reference the Daily Work Instructions for specific daily instructions.
3 .2 It is the responsibility ofthe Shih Supervisor to ensure that the procedure is followed and that any instructions that are r
· noted in the Daily Work instructions are also followed.
3.3 It is the responsibility ofthe Production Manager to maintain the procedure and to note any additional instructions in
` the Daily Work Instructions. The Production Manager is also responsible for reviewing testing and monitoring results
and forwarding completed and reviewed records to the Environmental Affairs Manager.
n 3 .4 It is the responsibility ofthe Environmental Affairs Manager to review and send reports to appropriate agencies and ile
- all records of testing/monitoring for their specified times as required by State and Federal rules and regulations.
6.0 fno canons " . h P ·
6. 6 S arnpling Requirements
` 6.6 .`l FPC-DE is requned to take specific effluent wastewater samples and conduct analytical testing by a certified
outside waste water laboratory. Routine sample schedule may change due to plant or lab scheduling. The
following is the NPDES required sampling and testing for TSS and BOD with its required frequency.
. _ . Annual parameter analysis is also completed on a composite sample. _ __
_ - _ 6.6.2 _ Weekly Sampling ‘ .
. 6.6.2. l _ P .24 H our Composite Sample ('A gallon, 1900 ml, sample) - ls taken every week from the Effluent
C T (001) of the Waste Water Treatment Plant, starting Monday morning at 9:00 and completed 9:00
Tuesday using the IS CO sampler. · ·
_ _ A 6.6.2.3 Outside Laboratory - Supplies containers for samples and picks them up on Tuesday aher 10:00
a.m. . .
l ‘ 6-7 Composite Sampling, Calculations and Logging `
. 6.7.1 Before starting composite sampling, acquire a Sample Data Sheet (Attachment Al) and fill out as follows: U
A) Check appropriate box for sampling to be taken. l l - P
B) Enter location of sample being taken (permitted plant effluent point is 001).
l C) Enter flow meter calibration factor. This factor is based on the flow meter calibration which is
· determined by Instrumentation department based on equipment in service. The flow meter is -
- located in the W WTP Control Room.
` D) "Total Flow" (in gallons) - Can only be entered after the composite is completed and the initial flow
P meter reading is subtracted hom the final flow meter reading and multiplied by the flow meter
_ calibration factor. ‘
E) "lnitial Flow Meter Reading" - Enter reading when composite sample is started. Also enter date,
time and Operator starting composite sample. _ `
F) "Final Flow Meter Reading" — Enter reading after last composite sample has beentaken. Also enter
date, time and Operator completing composite sample.
r G) "D ate" - Date that hours composite sample was taken. (Numbers down Erst column in numerical
MAINTAINED BY: Production Manager - REVISED DATE: 07/ l 5/O3 .
APPROVED BY: Plant Manager EFFECTIVE DATE: 08/14/96
Document is uncontrolled unless one ofthe fohowing appears; a red stamp stating “Cim1ro|1ed-D¤¤umerrt“ or “Revised·i)estroyAl1 Other Copies" or a red FPC logo inthe center ofthe page n n

Case 1 :05-cv-00443-G IVIS Docu ment 3-7 Filed 06/28/2005 Page 3 of 3
FPGDE FINAL EFFLUENT COMPOSITE SAMPLING AND _
FILE: XX_XXXX TESTING USED FOR WEEKLY NPDES SAIVEPLTNG Page 2 Oi`2
(Excerpted from FPC-DE Procedure OM269.0 10) ,
order, 1-25, indicates which hour of composite sample. Number 25 is for totaling, since a ·
_ composite sample only consists of 24 hours.)
, . H) "’l`irne" -- Time composite was taken. (
- I) "Total Flow this I—Iour" — Enter flow for that hour by subtracting hour one’s flow meter reading fiom
_ . hour two’ s reading and repeat for hour two by subtracting its reading from hour three ’s reading and
so on.
· J) "F1ow Meter Reading’° — Enter flow meter reading at beginning of each hour.
K) "Sample Size” - Will be calculated after 24th hour sample has been taken by following calculation
- at bottom of Sample Data Sheet. Reference Step of this section l ' -
L) _ "Operator l¤itials" — Enter initials of Operator who logged data for that hour.
M) "Caleulation to Determine 24-Hour Composite Sample Size" - This formula determines each hour`s
sample size based on overall sample needed and actual flow by: take 1900 ml (total sample size
- required for normal weekly composite which equals 1900 ml or % gallon) and divide it by the total
. hourly flow (all 24 hours total flow). Take this number 3 decimal places back from the decimal
point, ie. .051 and multiply this number by each hour’s total flow, giving you each hour’s sample
size (log in column "Sample Size.°’ See Step “L" of this section.)
l N) When the sample size has been determined the composite sample is made up using aliquots from _
_ each ISCO bottle. Vigorously shake each IS CO bottle then measure the correct amount into a
` graduated cylinder. Pour each aliquot into the % gallon sample bottle. ·
. _ O) "Sarnple Refrigerated -' Yes or No" - Rehigerate all samples unless otherwise stated. .
_ - P) "Sample Picked ·Up - Date, Time and By" — Enter the date, time and individual’s initials who -
I picked up the composite sample. Every sample picked up by an outside service requires a "Chain ”
. F ‘ of Custody Record" which is supplied by the service taking the sample. Check to confirm
- Y · information entered on "Chain.of Custody Record" is accurate, ie. proper sample description, _
analysis required, date, time and quantity .' Then sign of as relinquisher and sampler. After the
outside service representative has signed oil} make sure you retain a copy for our records.
MAlNl`AINED BY: Production Manager REVISED DATE; 07/ I5/03 e
APPROVED BY: Plant Manager EFFECTIVE DATE: 08/ 14/ 96
Documentis uncontrolled unless one ofthe following appears; arod stamp stating “C0ntmlledDoc11rnent“ or "R.evised-Destroy All Other Copier" ora red FPC logo in the center ofthe page