Free Opening Brief in Support - District Court of Delaware - Delaware

Case 1:04-cv—01507-SLR Document 270-5 Filed 07/06/2006 Page 1 of 4

a ik ’ Case 1:04-cv—01507-SLR Document 270-5 Filed 07/06/2006 Page 2 of 4 E
· , — 'D
D~·LIlTIOI1€l‘I€ As A D€gl‘63SII‘lg Agélll __ te Irrigation and
B ·· Frost Protection
·$ V ‘ on potential new uses lor this by~ .
{ RICHARD I-- °°LEMAN ¤r¤¤¤¤t..· stm d-Iirnoneng r, an ex. LOW 9¢0fy¢3
_ CllY¤$ and S¤b¥Y¤Pl¤¤l P'°d”°“ cellent solvent for grease and other cost c"‘cfr,rkc’I
’ i L3b¤|'B‘°|'Y· organic materials, its use as a degreas— Q i”c•
Wlm¤I’ H¤v¤¤.Fl¤ri¤¤ ing agent for machinery and as a ‘ at
waterless hand cleaner was explored. ‘ ‘ f
` Ab§l'°°l E The methods and results of this in— yi Ecrgei- gggoxfnam
l The r=<>¤¤¤¤I¤I ¤I d-I·¤·¤¤¤¤¤ I¤h¤ vestigation are the subject ot this _l7Ieaters:· ,M,,,,f£,‘LQ,,_E’ I
. principal component in orange cill as ,Bp¤,(_ ·;`=4 v`‘_v *;lQ'2’1'3_°§·g{2E2E .
a degreasing agent was explored. Commun} on page 24 -1 _P°E md `
D-Limonene was used in three lormu- an l
E V latiuns: a gel·type hand cleaner, a 1
Iotiorvtype hand cleaner and a gel- _ . ‘
\ typeengine cleaner. b 9 M
E Introduction O y I ! '
V ` Increasing recovery of distilled oils ‘ .
E (mostly d·lirnonenel by the citrus `
{ industry has prompted investigations
l .
. ‘Dne of the laboratories ol the Southern
l F¤¢9i¤¤. U. S. Dcnarlmertt ol Agriculture. B E
· Aqrlcuttural Research Servlce. ' -
k Mention ol brand names ls lor ldentlllcallan 0 I
only and does not lm¤ly endorsement bY - *
`_L the u. 5.. Department ot Agrlculture.
.; .
B y tl .
·I IRRlGATlON... 4-E E, I
It': Too CRlTlCAL · M ¥ - 7
r ' llll
And Costly Not To _________________ · lmélfiii I ,.,.¢__
.,,. E CD Th BEST Y ,,,, _ _ _ ._.» mn ;=!l www
ntact e A
S
sk our
l h I I `I USE BENZ-OLHLDIZ IN MY' LOMBNATION CROP
( C envca GJPRAYING-{SKY WIZJTING ACK IT SPELLG. our . . _
. E_ Supplléf eoovevra to Ate Krups on Mne·s."
I
F `q"i?”‘u§"°"‘ig) i BENZ-O-CHLOR 4-E miticide is an emulsifiable
·¤ - · -
- _ CENTER WOT solution containing 4 pounds ol chlorobenztlate l
_ • DRIP n `
i . me ver ¤¤"·>
• TRAVELlNG GUN
I rltltlulr e I e 0 W E R
MACHINERY C0. '_»: l an __ _ - ` .
a.w.R¤t.~S0~sT. I CH EM ICAL COM PANY
· om.Arwo,r=t.A.:t2e¤2 F H __ ‘a.,
(3051 4234474 a` I , · Montverde Road and S. C. L. Railroad .
J¤=¢¤h M- M¤N¤¤¤¤r¤.F-E-.Pr==i¤¤¤¤ T= __ , .... CLERMONT, FLORSDA 32711
'. Charter Member: ` ` · A lgggt 555.2333 `
t=¤.om¤A tnntoutow socterv
_ THE CITRUS INDUSTRY • November, l£l75 23
` ·‘·. T{T?F··;;i‘?.,sL‘2rii·}¥¥ '·'=` 5} ‘‘·._· —-Z¤?£E.¤1¥‘,`?'r.%‘·¢Q*€".°.a§:}&¥?*3iii-`??‘Zia?§é?`é`¥2·’:;·i>°¥=:¤t`»; =·}Q}i’ ·.

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‘ Ca` s‘e"l‘: -c - - D - ·· Fi|ed·07%06/2006 Page 3 of 4
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. ·-;·,` ;i§€=?+“F;;` -;:Ze¢·_¢‘*·;·’F%*:a-.L;·25 ;`,·, ‘.‘` .» R-
-. i';FJ'=Z = {--¥*‘·`·* ‘'‘· 5"·<,7"·lf.`-’·*»’*._·=¤ =°*"' ·»1»-€§<`v?’ **’·=..‘ °‘_4 ‘ E·"`?“;’ ‘`·*` ji;—‘·7~-;‘?€·‘3z?j··°-;-*_=;‘i.*$;."’:`.F£:?*.`] _·`. =_»-2 ·‘.· Isij.,
i Degreasjng solvent were prepared and evaluated as their hands. In other tests, they tounr
Continued 'mm Page 23 ;i;me•:;s Sgna/;;ea;t:g:A;\E;gi2;u;§: :::2 c;;rt;;no:‘ plogucfs to be. as effec
Q . · er » ceaners in remov
‘ _ _ QD N _ el-limonene as the rnaior component ing grease. sludges, lacquenlike resi
_ l D°°""°d Cimfs °'i ( 94'° d`i"T'°` were evaluated as engine cleaners. dues and other deposits that accumu ~
i nenei was °bm"°d fm"` a °h°m°Fa` In tests conducted by Lehning.5 he late on and in machinery during use
$"p°“°'2_ me "°°d in the i°u°`”'"g and his mechanics found the formula They expressed a definite prelerencr
. {°'m"i°"°"°‘ tions containing d~limonene equal to tor the citrus oil-containing Engg-,.
Q _ _ commercial waterless hand cleaners in
‘ S°Iu"°° A' Z ;:?;';£;°d loosening and removing grease' from Concluded on Page 25 ?
l00 9 Flenex 6903
‘ 5lO g d—limonene M I V` :_:
Solution B: 5.0 g sodium hydroxide " / / " Q,
3l5.0gwater .`_‘` 4
‘ instructions: Gradually heat solution "
A until the stearic acid melts, then QA. '·;__
cool to room temperature. Add solu·
tion B to A, mixing well until a gel Ti: f
forms ` · . .
. ‘ mklcr Irrr at: ,-;.
Lotion-Tyne hand cleaner Spr 9 On Equipment _;4i‘
Solution A: 300-450gd-limonene GHB Old Winter Garden Road
· Q aoglanatan ` ‘t:t ORLANDO, FLORIDA 32811 __
· Solution B: 25 g Arlacel 40:*
Q 759 Tween 403 _I__ h one l305) 293-555
l5g Arleeei ao= ` " ‘’**=~*·· · ·==·
_ BSQTWEEH 50:1 Charter Member Florida Irrigation Society
· " instructions: Mix solutions A and B, `
i then heat to 60°C. Heat 420~57O g of P` w
water to E2‘lC and mix with solution 4
Q (A + B). Stir moderately until the , ._. ?g n **4 :- "°°"* " Q
emulsion is cool. I (I 'l["""T`I"°`i`ii_I
Gel·Type Engine cleaner QR`: ...l _—
Q 500 g cl-limonene L g__ /Q-12s? Q
l00gGalac RM ——5‘l0‘ ` '
370 g water
i 30 g triethanolamine . Q
i Instructions: Boil the mixture. I _ Q 4 i
· RESULTS AND DISCUSSION
Q The gel and lotion hand cleaners }
I V . I
, incorporating dlimonme as me main , O KR 40 YEARS SERVICE TO THE CITRUS INDUSTRY r
. Q
{ ' Q ' Cilflll: Ffllll Dl'5lflblliDl’J‘ ' Chilled Citrus Section;
i Ask your , • Bulk Concentrate Sales und Processing ¤ Participation Plan.: ·
Chemical Supplier
V • Complete Grove Seniice ¤ Cash Fruit Bu yer:
Q About. . ._ TM
i . . p"0"Cl D B. C. Cook Et Sons Enterprises, Inc.
i Florida Made for the Agri-Trade _._4 Q_ »~·» __ i
l L 413 N, 12lh Street ·‘t_Q Haines City, Florida 33844 l
r TOWER P. 0. aux tser 1 A-’ Phone: B13/422-Jl2I
` cuemncm. company ~ i
.; M cl Rdi d SCL I ( I 4
®§ E CL;r;::3;T' FS132711 Affiliated ;it:lGr:ge;·s Psscezsing Service
_ (305) 6564333 Ig an yl on B
I 24 THE CITRUS INDUSTRY • Nuvember. 1575
1 LPM 000208 Q 1

; ‘ Case 1 :04-cv—01507-SER Document 270-5 Filed 07/06/2006 Page 4 of 4 ;
. ‘
"’ 34 _.’ Applicants Wanted For Harvesting Incentive Plans
c· . ‘ i
{L
Yr Specialty or "zipper skin" fruit mended rate_" Blair said. "We'vt: $30,000 set. Incentive rates under
It wl. varieties represent a maior harvesting budgeted $50,000 for the incentive this plan will be determined on an
E problem lor the Florida citrus industry program." individual cooperator basis.
_; but a new incentive plan being recom- The committee also approved two Blair explained that the entire
Q mended by the Florida citrus harvest- other plans lor recommendation to the research and development effort must `
E ing research and development commit- Commission that arc designed to epa be based on "reliahle data _that will
tee may prove that the job can be courage mechanical harvesting opera- reveal a system'; efficiency and com-
madeeasier. tions and provide crucial data. A meruialfeasibility." ,
` Terms ol the plan call for the research plan to gain data important A mechanical harvesting incentive `
Florida Citrus Commission to share 50 to the industry's overall ellort was
` _ per cent of the costofabscissiori agents recommended and a budget ol Concluded on Page 25 ,
· 0,. {mn inosengng Chemicals used 0,, ~
° truit that will be harvested by hand. _ _ _ _ v_ I H _ _
, Jim Blair, or the Florida Depart- ir?. ;-.* .~-' ‘--`· ij! ·‘‘-.`, {2* l-,'
ment of Citrus and coordinator or the if N ._ R O F I
' research and development elfort, said ;_-;j1_:.v-; ,;g,; r_;-;i‘_§·ig=t-jY_ .=*_ , .._- 2 ·‘·_l. g,;.._.; __;¤·-f1_.=;-.{;=g: ‘·-_ , -.». -. 5, _ V
Itarvestors and growers interested in i' L A -Q,4»·°i’*`Y‘.‘v’j°]_;;€i· - i` ` `.`· M In ll . `_4.' _'_`
taking advantage ol the incentive __
should contact him immediately for ` _ n n 4 _ _ " " A A _ _ "
appucadcmd This wonderfully delicious fruit offers unusually high profits
,.Each cccpcrawr can receive upto to the capable grower. For information about top quality
me rawara ala was or chemicals, elm ='*t¤¤ item New Z¤¤'¤¤¤· Write ·¤
applied at the manulacturefs recom· BRAMEN COMPANYr |Nc— D¤P*· Cl -
P. O. Box 70 Salem, Mass. 01970
Degreasing
Continued from Page 24 · _
r cleaner because it caused less skin
'rritation and had a m e leasant i
‘d P . from Melanosclireasy Spot,
o or than the commercially available · •
mia. cleaners. Brown Rot and Cntrus Scab
. 3 .
Thus, the d-limonene-containing
hand cleaners were as effective as
commercially available waterless hand ‘
cleaners. As engine cleaners, d·limo· ° C S f
nene·containing gel and liquid had two _
` l advantages over commercial degreas~ _
ers, a pleasant odor and caused less
skin irritation. Further information
‘ may be obtained by contacting the ..,;;,;f` if ·''=· 9-;;- _;
U. S. Citrus and subtropical Products _ ·"
` . f. r {V · *‘ \ `-
Laboratory, P. O. Box 1909. Winter __,;;.,·. Wy ._ hr » J;. _
never., Florida azaao. ,.a, 1 ;- ii ._ * _ 2
f; _ I . ,.2 ti;::;·—_ ·‘i M
ruzr=t-znences L ' `
I. Coleman. R. L. and P. E. Shaw. IS74.
Potential uses nl some dlstltlen oils. CII-
rut lndustry 55(2t:2o..
2. FI lun chemical cn., t . Lake Alt ed, ·
"' ' dodge
1. Rene: 590. Ari el 40, T m 40. · -
Arson! ED and Twain 80 are“:nulsHy· Mn/ng cnlpulwuun {7 as,. _
lng agents purchased Irom Allan Chem- 2¤¤*‘¤’· A••·M.N•••V°'\.NV WU77 `· ~ _E\ ‘ 4\ . :· ~._ . vp,
‘ test tneustriu. inc., Wllmlngton, om- *"'*"‘”°° "·. `:-p` -` eQ%·I p ‘§“’
wan. HUB!. ”§~ L" .` - ·f”!’¤
4, Gala: RM·Sl¤ Il an ernutsllylng agent ,'t` EQ " ;§
purchased from General Anlllne Film `·‘·'=` -~< .t· 'V 6 @
corp., M0 West Stat, New Vork, New .
York t0¤20. _
' s. Mr. Lester canning, Me¤r•ant¤·ln·criaroe. Also Producers of Pontohydrnto Coppor Sulfoto ·Solomum· Copper Oxide
;::‘;:":':;“':::;::"I;":: °“°· F'°'l°‘· Bc certain that tha product you buy is registered with EPA
THE CITRUS INDUSTRY • November. l575 25

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I LPM 000209
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